Free Access
| Issue |
Microsc. Microanal. Microstruct.
Volume 6, Number 2, April 1995
|
|
|---|---|---|
| Page(s) | 237 - 248 | |
| DOI | https://doi.org/10.1051/mmm:1995120 | |
Microsc. Microanal. Microstruct. 6, 237-248 (1995)
DOI: 10.1051/mmm:1995120
CRMC2-CNRS, Campus de Luminy, Case 913,13288 Marseille Cedex 9, France
8110B - Growth from vapor.
8107B - Nanocrystalline materials.
6855J - Structure and morphology; thickness; crystalline orientation and texture.
Key words
Experimental study -- Crystal growth from vapors -- Ultrahigh vacuum -- Vapor condensation -- Particles -- Palladium -- Catalysts -- TEM -- High-resolution methods -- Orientation relation -- Crystal orientation -- Heteroepitaxy -- Zinc oxides -- Binary compounds -- Surfaces -- Interfaces -- Condensed matter physics -- Materials science -- Physics -- Metals -- Metallurgy -- Condensed state physics -- Transition elements -- Inorganic compounds -- Transition element compounds
© EDP Sciences 1995
DOI: 10.1051/mmm:1995120
HRTEM Studies of the Epitaxial Growth of Pd Particles (1-6 nm) on ZnO Micro-Prisms
Suzanne Giorgio, Claude R. Henry et Claude ChaponCRMC2-CNRS, Campus de Luminy, Case 913,13288 Marseille Cedex 9, France
Abstract
Pd particles (1-6 nm) were grown under UHV conditions
from a Knudsen
cell, on small ZnO prisms in situ prepared in a controlled
atmosphere. 3-D Pd particles epitaxially oriented on the ZnO
faces were observed by HRTEM, both in top view and in profile
view on the lateral (10.0) faces of the ZnO prisms. The
epitaxial relations were determined:
and
![$\rm [011]_{Pd}\parallel [001]_{ZnO}$](/articles/mmm/abs/1995/02/mmm_1995__6_2_237_0/img2.gif){kind=small}
. From the HRTEM observations
of the single
ZnO prisms and the tetrapods twins, the precise structure of the
central ZnO nucleus was also evidenced.
8110B - Growth from vapor.
8107B - Nanocrystalline materials.
6855J - Structure and morphology; thickness; crystalline orientation and texture.
Key words
Experimental study -- Crystal growth from vapors -- Ultrahigh vacuum -- Vapor condensation -- Particles -- Palladium -- Catalysts -- TEM -- High-resolution methods -- Orientation relation -- Crystal orientation -- Heteroepitaxy -- Zinc oxides -- Binary compounds -- Surfaces -- Interfaces -- Condensed matter physics -- Materials science -- Physics -- Metals -- Metallurgy -- Condensed state physics -- Transition elements -- Inorganic compounds -- Transition element compounds
© EDP Sciences 1995